B() Standard Test Method for Measurement of Coating Thickness by X-Ray Spectrometry coating thickness~ Format, Pages, Price. PDF. This standard is issued under the fixed designation B; the number 1 This test method is under the jurisdiction of ASTM Committee B08 on Metallic. ASTM B Standard Test Method for Measurement of Coating Thickness by X- Ray Spectrometry. One of the biggest issues in critical bolting operations is.
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astm b pdf famu lady info, astm b standard test method for measurement of, astm b 98 techstreet, astm b radiation views, astm b x. ASTM B - Designation: B – 98 (Reapproved ) UNCONTROLLED (if printed out) Standar. Sign In · View Account▹ · Home; ASTM B() $; Add to Cart. Printed Edition + PDF; Immediate download; $; Add to Cart.
The value should not be signi? Some forms of instability become evident if the same specimen is measured periodically.
Operation of the gas-? Instrument measurement precision will rapidly decrease with increasing thickness in the hyperbolic range. For this reason, signi? Calibration 7.
Standards representing various thickness ranges of a number of coatings on different substrates are generally available from thickness gage manufacturers. Those that are certi? Calibration standards for gold coatings, certi? If the standards are visibly scratched or abraded they should be replaced. It is recommended that two sets of standards be maintained, that is, a set of primary standards and a set of working standards. These should be used only to calibrate and periodically check the condition of the working standards.
At the? Exceptions are allowed if the intensity of the characteristic coating material emission is not in? An example of this situation is the measurement of silver on copper. The instrument calibration may be made with standards of silver on nickel.
The intensity of the characteristic silver emission is not in? If the coating of the standards is electrodeposited from the same bath and under the same conditions as the coating to be measured, the X-ray properties may be assumed to be the same.
If the coating on the standard is gold, but not electroplated under conditions known to be the same as the coating being measured, the X-ray properties may be assumed to be the same for mass per unit area measurements. Under such circumstances, thickness measurements must be corrected for density differences, unless density differences can be shown to be insigni? This shall be veri? This standard less measurement shall be corrected by means of calibration standards.
The standards correction procedure calibration performs the same way as the procedure used for establishing empirical instrument calibrations alone. Referee Test 9. The SRM shall be measured? If the average of the? The stated mass per unit area of each coating thickness SRM is certi?
Procedure Calibrate it in accordance with Section 7.
If there is a change of the measured thickness that is large enough to preclude meeting the requirements of Section 11, recalibrate the instrument. If not, make sure that the calibration has been made with a substrate having the same thickness and emission properties as the test specimens. In no case shall the measurement area be larger than the coated area available on the test specimen. Suitable means must be provided to perfectly align the test specimen relative to the excitation beam.
Avoid specimen areas having visible defects such as? The conversion is made automatically by most commercial coating thickness instruments. Precision and Bias It is, therefore, no greater than, and attributable to: 1 the calibration error of the instrument, and 2 the quality of the calibration standard used to calibrate the instrument.
Report Keywords However, the general shapes of calibration curves in the emission mode and in the absorption mode of operation are given here as general information. The intensities are background-corrected, that is, the intensity for Ni Ka is obtained from a sample of the unplated brass substrate and subsequently substracted for each of the intensity readings obtained from electroplated samples.
The intensities are background-corrected as they were in the emission technique. The emission now being measured comes from the substrate. Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility. This standard is subject to revision at any time by the responsible technical committee and must be reviewed every?
Your comments are invited either for revision of this standard or for additional standards and should be addressed to ASTM International Headquarters. Your comments will receive careful consideration at a meeting of the responsible technical committee, which you may attend. If you feel that your comments have not received a fair hearing you should make your views known to the ASTM Committee on Standards, at the address shown below. However, that cost can be much greater if an organization neglects early warning signs or avoids preventative maintenance.
These electronic components can short out internally, creating heat and a burning effect. Obviously, additional component damage will increase repair costs and may extend the downtime.
Fortunately, these extreme situations can be avoided with awareness and early action. Pre-determined hours will vary based on the tube plus a number of additional — controllable — variables.
The environment that an XRF analyzer is in, the amount an XRF is used ie single shift, double, etc , the collimator sizes used, and the applications can all factor into if the component lasts longer or less than the expected lifespan.
Learn More! What Routine Service Can Do As an x-ray fluorescence owner, your organization should have a routine certification and safety radiation service performed by an Accredited XRF service organization. When performed by Eastern Applied, this service would also include preventative maintenance and best practices consultation.
Service technicians from Eastern Applied Research are instructed to review the variables that affect x-ray tube life and other major components , advising clients on operational or environmental adjustments to consider while also discussing what a realistic life span remaining is for major components.
Exceptions are allowed if the intensity of the characteristic coating material emission is not in? It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
If there is a change of the measured thickness that is large enough to preclude meeting the requirements of Section 11, recalibrate the instrument. The precision rapidly becomes poorer in the portion of the curve above approximately 10? The value should not be signi?
Typical examples of such combinations are gold on nickel on copper and nickel on copper on steel. It also provides an overview of calibration techniques and best practices along with standard-less fundamental parameters calibrations.
The conversion is made automatically by most commercial coating thickness instruments. These should be used only to calibrate and periodically check the condition of the working standards. To understand the signi? The intensities are background-corrected, that is, the intensity for Ni Ka is obtained from a sample of the unplated brass substrate and subsequently substracted for each of the intensity readings obtained from electroplated samples.
This industry standard ASTM B should be reviewed by all operators of x-ray fluorescence because it offers a beneficial overview and highlights proper implementation of the technology.
It is recommended that two sets of standards asttm maintained, that is, a set of primary standards and a set of working standards. This does not mean that the result would necessarily be ten times as accurate see 7. For this reason, signi?
This is because both the exciting and secondary characteristic radiations undergo attenuation in passing through the coating.